TA Instruments

AR1706-0001f

04/09/2012 16:26:40

Sample name	ASW 10 mm from base, 60 mm to top, disk 18 PMMA+FA fouled AND CLEANED
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1706
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 16:26:40

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-24.54	5.887	-4.169	1.0000	22.4	611.7	2.5989	10000	0.1501	17.65	3.2486	324.86	3.384E-3	0.0	1.0	61.000	-75.288	4.710
0.7208	12.68	0.05684	2.0200	22.4	607.6	13.6998	10000	0.1491	3.779	17.125	1712.5	3.384E-3	0.0	1.0	62.020	2.2114	10.14
1.527	19.54	0.07817	3.0160	22.4	611.7	27.3590	10000	0.1501	1.603	34.199	3419.9	3.384E-3	0.1	1.1	63.016	4.6851	15.63
2.095	23.18	0.09038	4.0240	22.4	608.4	42.2512	10000	0.1493	1.132	52.814	5281.4	3.384E-3	0.1	1.1	64.024	6.4275	18.54
3.367	30.90	0.1089	5.0160	22.4	610.9	67.8709	10000	0.1499	0.6397	84.839	8483.9	3.384E-3	0.1	1.1	65.016	10.329	24.72
5.127	39.53	0.1297	6.0160	22.4	625.0	107.5720	10000	0.1534	0.3999	134.47	13447	3.383E-3	0.1	1.1	66.016	15.728	31.62
5.797	42.57	0.1362	7.0120	22.4	611.7	126.7570	10000	0.1501	0.3375	158.45	15845	3.383E-3	0.1	1.1	67.012	17.784	34.06
7.275	49.15	0.1480	8.0160	22.4	616.7	165.3910	10000	0.1514	0.2552	206.74	20674	3.384E-3	0.1	1.1	68.016	22.321	39.32
9.768	57.56	0.1697	9.0160	22.4	605.9	223.6440	10000	0.1487	0.1829	279.56	27956	3.383E-3	0.2	1.2	69.016	29.969	46.05
11.80	63.71	0.1852	10.016	22.4	612.5	274.8440	10000	0.1503	0.1509	343.56	34356	3.384E-3	0.2	1.2	70.016	36.203	50.97
13.64	69.67	0.1958	11.016	22.4	615.9	326.1840	10000	0.1512	0.1269	407.73	40773	3.383E-3	0.2	1.2	71.016	41.844	55.73
15.61	75.14	0.2077	12.016	22.4	611.7	377.3340	10000	0.1501	0.1084	471.67	47167	3.383E-3	0.2	1.2	72.016	47.887	60.11
17.24	80.53	0.2141	13.000	22.4	599.3	435.1380	10000	0.1471	0.09242	543.92	54392	3.384E-3	0.2	1.2	73.000	52.883	64.42
19.54	86.44	0.2260	14.000	22.4	610.1	498.7500	10000	0.1497	0.08164	623.44	62344	3.383E-3	0.2	1.2	74.000	59.937	69.16
22.53	94.61	0.2381	15.016	22.4	601.0	594.3090	10000	0.1475	0.06713	742.89	74289	3.384E-3	0.3	1.3	75.016	69.112	75.69
24.96	99.92	0.2498	16.016	22.4	594.4	664.3570	10000	0.1459	0.05953	830.45	83045	3.383E-3	0.3	1.3	76.016	76.580	79.94
27.07	105.7	0.2562	17.004	22.4	588.6	740.8140	10000	0.1445	0.05271	926.02	92602	3.384E-3	0.3	1.3	77.004	83.053	84.54
30.58	113.7	0.2689	18.004	22.4	593.5	855.1370	10000	0.1457	0.04588	1068.9	1.0689E5	3.384E-3	0.3	1.3	78.004	93.821	90.99
32.43	118.8	0.2730	19.016	22.4	596.0	931.3340	10000	0.1463	0.04223	1164.2	1.1642E5	3.384E-3	0.3	1.3	79.016	99.492	95.05
34.92	124.3	0.2810	20.020	22.4	581.1	1020.9000	10000	0.1426	0.03764	1276.1	1.2761E5	3.384E-3	0.3	1.3	80.020	107.13	99.41
38.67	132.3	0.2923	21.016	22.4	579.5	1153.9500	10000	0.1422	0.03311	1442.4	1.4424E5	3.384E-3	0.4	1.4	81.016	118.65	105.8
40.79	137.4	0.2969	22.016	22.4	583.6	1242.2100	10000	0.1432	0.03092	1552.8	1.5528E5	3.384E-3	0.4	1.4	82.016	125.16	109.9
43.02	142.8	0.3012	23.016	22.4	586.1	1343.7200	10000	0.1438	0.02874	1679.7	1.6797E5	3.384E-3	0.4	1.4	83.016	131.98	114.2
47.72	150.8	0.3164	24.016	22.4	575.3	1495.7400	10000	0.1412	0.02529	1869.7	1.8697E5	3.384E-3	0.4	1.4	84.016	146.41	120.7
50.52	155.9	0.3240	25.016	22.4	560.5	1597.0400	10000	0.1376	0.02305	1996.3	1.9963E5	3.384E-3	0.4	1.4	85.016	154.99	124.7
53.55	161.3	0.3319	26.016	22.4	548.9	1711.1600	10000	0.1347	0.02109	2139.0	2.1390E5	3.384E-3	0.4	1.4	86.016	164.28	129.1
57.49	169.3	0.3395	27.000	22.4	570.4	1882.0300	10000	0.1400	0.01989	2352.5	2.3525E5	3.384E-3	0.5	1.5	87.000	176.39	135.5
60.27	174.5	0.3455	28.016	22.4	554.7	1996.0500	10000	0.1361	0.01823	2495.1	2.4951E5	3.384E-3	0.5	1.5	88.016	184.90	139.6
62.95	179.6	0.3506	29.016	22.4	547.2	2116.2400	10000	0.1343	0.01697	2645.3	2.6453E5	3.383E-3	0.5	1.5	89.016	193.12	143.6
68.19	187.6	0.3635	30.000	22.4	555.5	2306.0000	10000	0.1363	0.01579	2882.5	2.8825E5	3.383E-3	0.5	1.5	90.000	209.19	150.1
71.20	192.7	0.3695	31.000	22.4	543.9	2433.2900	10000	0.1335	0.01465	3041.6	3.0416E5	3.384E-3	0.5	1.5	91.000	218.44	154.2
75.32	200.5	0.3756	32.020	22.4	553.0	2636.2000	10000	0.1357	0.01375	3295.3	3.2953E5	3.384E-3	0.5	1.5	92.020	231.09	160.4
77.98	205.8	0.3789	33.012	22.4	520.0	2773.9299	10000	0.1276	0.01227	3467.4	3.4674E5	3.384E-3	0.6	1.6	93.012	239.25	164.7
82.97	211.0	0.3932	34.016	22.4	528.2	2912.8799	10000	0.1296	0.01187	3641.1	3.6411E5	3.384E-3	0.6	1.6	94.016	254.54	168.8
87.19	218.6	0.3988	35.016	22.4	515.0	3127.8999	10000	0.1264	0.01078	3909.9	3.9099E5	3.384E-3	0.6	1.6	95.016	267.48	174.9
90.75	223.9	0.4053	36.004	22.4	519.1	3282.3000	10000	0.1274	0.01036	4102.9	4.1029E5	3.384E-3	0.6	1.6	96.004	278.42	179.1
94.04	229.1	0.4105	37.000	22.4	525.8	3431.5901	10000	0.1290	0.01002	4289.5	4.2895E5	3.384E-3	0.6	1.6	97.000	288.51	183.3
98.47	236.6	0.4161	38.016	22.4	525.8	3659.1699	10000	0.1290	9.389E-3	4574.0	4.5740E5	3.384E-3	0.6	1.6	98.016	302.09	189.3
102.6	241.8	0.4242	39.020	22.4	514.2	3823.0000	10000	0.1262	8.792E-3	4778.8	4.7788E5	3.384E-3	0.7	1.7	99.020	314.70	193.5
106.4	249.6	0.4265	40.024	22.4	520.0	4069.7600	10000	0.1276	8.347E-3	5087.2	5.0872E5	3.384E-3	0.7	1.7	100.024	326.54	199.7
110.5	254.6	0.4339	41.020	22.4	518.3	4233.8301	10000	0.1272	7.995E-3	5292.3	5.2923E5	3.384E-3	0.7	1.7	101.020	338.97	203.7
114.7	259.8	0.4413	42.000	22.4	497.6	4409.4800	10000	0.1221	7.371E-3	5511.9	5.5119E5	3.384E-3	0.7	1.7	102.000	351.82	207.9
121.0	267.6	0.4521	42.996	22.4	501.0	4674.6201	10000	0.1230	6.995E-3	5843.3	5.8433E5	3.383E-3	0.7	1.7	102.996	371.18	214.1
123.2	272.7	0.4520	44.000	22.4	499.3	4851.2598	10000	0.1225	6.716E-3	6064.1	6.0641E5	3.383E-3	0.7	1.7	104.000	378.09	218.1
129.4	280.4	0.4614	45.060	22.4	498.5	5129.1802	10000	0.1223	6.342E-3	6411.5	6.4115E5	3.384E-3	0.8	1.8	105.060	396.85	224.3
133.1	285.5	0.4661	46.020	22.4	473.7	5318.3301	10000	0.1163	5.810E-3	6647.9	6.6479E5	3.384E-3	0.8	1.8	106.020	408.28	228.4
138.8	293.1	0.4735	47.000	22.4	468.7	5602.1602	10000	0.1150	5.456E-3	7002.7	7.0027E5	3.384E-3	0.8	1.8	107.000	425.77	234.5
141.2	298.2	0.4736	48.000	22.4	508.4	5797.6602	10000	0.1248	5.719E-3	7247.1	7.2471E5	3.384E-3	0.8	1.8	108.000	433.17	238.5
148.1	305.9	0.4840	49.044	22.4	489.4	6101.6401	10000	0.1201	5.230E-3	7627.1	7.6271E5	3.384E-3	0.8	1.8	109.044	454.24	244.7
152.9	311.0	0.4917	50.044	22.4	472.8	6307.0498	10000	0.1161	4.890E-3	7883.8	7.8838E5	3.384E-3	0.8	1.8	110.044	469.08	248.8
155.6	316.0	0.4925	51.008	22.4	454.7	6514.6499	10000	0.1116	4.553E-3	8143.3	8.1433E5	3.384E-3	0.9	1.9	111.008	477.47	252.8
163.2	323.8	0.5039	52.016	22.4	454.7	6832.1602	10000	0.1116	4.337E-3	8540.2	8.5402E5	3.384E-3	0.9	1.9	112.016	500.60	259.0
167.7	328.9	0.5101	52.996	22.4	471.2	7046.5200	10000	0.1156	4.357E-3	8808.2	8.8082E5	3.384E-3	0.9	1.9	112.996	514.65	263.1
172.9	336.4	0.5140	54.016	22.4	464.6	7374.4502	10000	0.1140	4.105E-3	9218.1	9.2181E5	3.384E-3	0.9	1.9	114.016	530.46	269.1
181.0	341.6	0.5299	55.024	22.4	427.4	7603.1299	10000	0.1049	3.663E-3	9503.9	9.5039E5	3.384E-3	0.9	1.9	115.024	555.31	273.3
182.0	346.7	0.5248	56.024	22.4	425.7	7943.9399	10000	0.1045	3.541E-3	9929.9	9.9299E5	3.383E-3	0.9	1.9	116.024	558.26	277.4
189.7	354.2	0.5355	57.000	22.4	419.1	8168.9199	10000	0.1029	3.340E-3	10211	1.0211E6	3.384E-3	1.0	2.0	117.000	581.97	283.4
193.3	359.3	0.5378	58.032	22.4	436.5	8408.7598	10000	0.1071	3.380E-3	10511	1.0511E6	3.384E-3	1.0	2.0	118.032	592.94	287.5
198.9	367.0	0.5420	59.016	22.4	409.2	8767.8896	10000	0.1004	3.038E-3	10960	1.0960E6	3.384E-3	1.0	2.0	119.016	610.22	293.6
205.5	372.0	0.5523	60.016	22.4	414.2	9007.2598	10000	0.1016	2.993E-3	11259	1.1259E6	3.384E-3	1.0	2.0	120.016	630.35	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

210.0	375.0	0.5600	1.0200	22.4	406.7	267.0720	10000	0.09982	2.892E-3	333.84	33384	3.384E-3	0.0	2.0	122.020	644.25	300.0
204.5	375.0	0.5453	2.0080	22.4	421.6	518.1690	10000	0.1035	2.998E-3	647.71	64771	3.384E-3	0.0	2.1	123.008	627.42	300.0
207.4	375.0	0.5530	3.0240	22.4	408.4	896.6740	10000	0.1002	2.904E-3	1120.8	1.1208E5	3.384E-3	0.1	2.1	124.024	636.26	300.0
207.4	375.0	0.5532	4.0120	22.4	441.4	1145.1600	10000	0.1083	3.139E-3	1431.5	1.4315E5	3.383E-3	0.1	2.1	125.012	636.40	300.0
209.3	375.0	0.5582	5.0240	22.4	392.7	1524.2400	10000	0.09637	2.792E-3	1905.3	1.9053E5	3.383E-3	0.1	2.1	126.024	642.16	300.0
207.5	375.0	0.5532	6.0120	22.4	403.4	1773.4301	10000	0.09901	2.868E-3	2216.8	2.2168E5	3.384E-3	0.1	2.1	127.012	636.46	300.0
210.6	375.0	0.5616	7.0080	22.4	403.4	2026.0900	10000	0.09901	2.869E-3	2532.6	2.5326E5	3.383E-3	0.1	2.1	128.008	646.14	300.0
207.9	375.0	0.5545	8.0080	22.4	425.7	2401.9600	10000	0.1045	3.027E-3	3002.5	3.0025E5	3.384E-3	0.1	2.2	129.008	637.92	300.0
204.7	375.0	0.5459	9.0120	22.4	439.0	2654.4700	10000	0.1077	3.122E-3	3318.1	3.3181E5	3.384E-3	0.2	2.2	130.012	628.00	300.0
208.1	375.0	0.5550	10.020	22.4	407.5	3030.4700	10000	0.1000	2.898E-3	3788.1	3.7881E5	3.383E-3	0.2	2.2	131.020	638.47	300.0
208.8	375.0	0.5567	11.028	22.4	389.4	3281.4099	10000	0.09556	2.769E-3	4101.8	4.1018E5	3.384E-3	0.2	2.2	132.028	640.49	300.0
209.2	375.0	0.5578	12.016	22.4	399.3	3532.6799	10000	0.09800	2.839E-3	4415.9	4.4159E5	3.383E-3	0.2	2.2	133.016	641.68	300.0
206.8	375.0	0.5514	13.008	22.4	433.2	3909.8899	10000	0.1063	3.080E-3	4887.4	4.8874E5	3.384E-3	0.2	2.2	134.008	634.44	300.0
209.6	375.0	0.5589	14.008	22.4	395.1	4161.1699	10000	0.09698	2.810E-3	5201.5	5.2015E5	3.384E-3	0.2	2.3	135.008	643.03	300.0
208.9	375.0	0.5572	15.008	22.4	400.1	4412.4302	10000	0.09820	2.845E-3	5515.5	5.5155E5	3.383E-3	0.3	2.3	136.008	641.01	300.0
208.3	375.0	0.5554	16.008	22.4	412.5	4794.2700	10000	0.1012	2.933E-3	5992.8	5.9928E5	3.383E-3	0.3	2.3	137.008	638.99	300.0
210.6	375.0	0.5616	17.020	22.4	405.1	5040.7998	10000	0.09942	2.880E-3	6301.0	6.3010E5	3.383E-3	0.3	2.3	138.020	646.08	300.0
204.2	375.0	0.5445	18.008	22.4	432.3	5417.6802	10000	0.1061	3.074E-3	6772.1	6.7721E5	3.383E-3	0.3	2.3	139.008	626.43	300.0
206.8	375.0	0.5515	19.008	22.4	413.3	5669.1602	10000	0.1014	2.939E-3	7086.5	7.0865E5	3.384E-3	0.3	2.3	140.008	634.52	300.0
205.9	375.0	0.5491	20.008	22.4	448.0	5920.4800	10000	0.1100	3.186E-3	7400.6	7.4006E5	3.383E-3	0.3	2.4	141.008	631.70	300.0
207.3	375.0	0.5527	21.024	22.4	400.9	6297.3999	10000	0.09840	2.851E-3	7871.8	7.8718E5	3.383E-3	0.4	2.4	142.024	635.89	300.0
205.6	375.0	0.5482	22.024	22.4	431.5	6549.0698	10000	0.1059	3.068E-3	8186.3	8.1863E5	3.383E-3	0.4	2.4	143.024	630.69	300.0
207.9	375.0	0.5543	23.036	22.4	418.3	6925.7402	10000	0.1027	2.975E-3	8657.2	8.6572E5	3.383E-3	0.4	2.4	144.036	637.71	300.0
208.1	375.0	0.5550	24.008	22.4	451.4	7177.0698	10000	0.1108	3.210E-3	8971.3	8.9713E5	3.383E-3	0.4	2.4	145.008	638.50	300.0
209.5	375.0	0.5588	25.008	22.4	404.2	7429.7202	10000	0.09921	2.875E-3	9287.2	9.2872E5	3.383E-3	0.4	2.4	146.008	642.81	300.0
209.9	375.0	0.5598	26.008	22.4	411.7	7806.6401	10000	0.1010	2.928E-3	9758.3	9.7583E5	3.383E-3	0.4	2.5	147.008	644.05	300.0
207.2	375.0	0.5524	27.020	22.4	426.6	8058.7002	10000	0.1047	3.033E-3	10073	1.0073E6	3.384E-3	0.5	2.5	148.020	635.55	300.0
206.8	375.0	0.5514	28.008	22.4	448.9	8435.4199	10000	0.1102	3.192E-3	10544	1.0544E6	3.383E-3	0.5	2.5	149.008	634.40	300.0
207.8	375.0	0.5541	29.348	22.4	421.6	8814.9102	10000	0.1035	2.998E-3	11019	1.1019E6	3.383E-3	0.5	2.5	150.348	637.48	300.0
208.2	375.0	0.5552	30.008	22.4	428.2	8936.4004	10000	0.1051	3.045E-3	11171	1.1171E6	3.384E-3	0.5	2.5	151.008	638.68	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

206.4	372.2	0.5544	0.99600	22.4	399.3	213.6740	10000	0.09800	2.882E-3	267.09	26709	3.384E-3	0.0	2.5	151.996	633.18	297.8
198.5	364.7	0.5442	2.0120	22.4	417.5	570.6980	10000	0.1025	3.139E-3	713.37	71337	3.384E-3	0.0	2.6	153.012	608.89	291.8
195.7	359.6	0.5442	2.9960	22.4	430.7	808.6820	10000	0.1057	3.330E-3	1010.9	1.0109E5	3.383E-3	0.0	2.6	153.996	600.40	287.7
186.8	351.9	0.5307	4.0040	22.4	467.9	1159.4301	10000	0.1148	3.778E-3	1449.3	1.4493E5	3.384E-3	0.1	2.6	155.004	573.00	281.5
184.6	346.9	0.5322	5.0000	22.4	449.7	1384.6300	10000	0.1104	3.737E-3	1730.8	1.7308E5	3.384E-3	0.1	2.6	156.000	566.43	277.5
180.2	339.3	0.5312	5.9960	22.4	448.9	1722.9200	10000	0.1102	3.899E-3	2153.7	2.1537E5	3.384E-3	0.1	2.6	156.996	552.99	271.4
172.4	334.1	0.5159	6.9960	22.4	471.2	1948.2800	10000	0.1156	4.221E-3	2435.4	2.4354E5	3.384E-3	0.1	2.6	157.996	528.80	267.3
167.1	329.1	0.5079	7.9960	22.4	468.7	2161.0500	10000	0.1150	4.328E-3	2701.3	2.7013E5	3.384E-3	0.1	2.6	158.996	512.76	263.3
162.9	321.5	0.5066	9.0400	22.4	461.3	2480.3799	10000	0.1132	4.463E-3	3100.5	3.1005E5	3.384E-3	0.2	2.7	160.040	499.68	257.2
157.6	316.3	0.4984	10.000	22.4	464.6	2693.2200	10000	0.1140	4.643E-3	3366.5	3.3665E5	3.384E-3	0.2	2.7	161.000	483.66	253.1
151.1	308.7	0.4894	11.000	22.4	462.9	2999.8701	10000	0.1136	4.859E-3	3749.8	3.7498E5	3.384E-3	0.2	2.7	162.000	463.48	246.9
146.5	303.6	0.4825	11.996	22.4	463.8	3201.0701	10000	0.1138	5.032E-3	4001.3	4.0013E5	3.384E-3	0.2	2.7	162.996	449.35	242.9
143.5	298.4	0.4807	12.996	22.4	481.1	3501.9700	10000	0.1181	5.402E-3	4377.5	4.3775E5	3.384E-3	0.2	2.7	163.996	440.12	238.8
138.4	290.8	0.4758	14.000	22.4	475.3	3688.2400	10000	0.1167	5.620E-3	4610.3	4.6103E5	3.384E-3	0.2	2.8	165.000	424.51	232.7
133.0	285.8	0.4655	15.000	22.4	472.8	3877.1699	10000	0.1161	5.790E-3	4846.5	4.8465E5	3.384E-3	0.3	2.8	166.000	408.09	228.6
128.8	278.0	0.4631	15.996	22.4	482.8	4157.3999	10000	0.1185	6.244E-3	5196.8	5.1968E5	3.384E-3	0.3	2.8	166.996	395.07	222.4
125.1	272.9	0.4586	16.996	22.4	497.6	4339.9902	10000	0.1221	6.683E-3	5425.0	5.4250E5	3.384E-3	0.3	2.8	167.996	383.91	218.3
118.8	265.3	0.4479	17.996	22.4	501.8	4601.5498	10000	0.1232	7.128E-3	5751.9	5.7519E5	3.383E-3	0.3	2.8	168.996	364.57	212.3
115.6	260.2	0.4444	19.012	22.4	518.3	4778.1201	10000	0.1272	7.658E-3	5972.7	5.9727E5	3.384E-3	0.3	2.8	170.012	354.70	208.1
111.4	254.9	0.4370	19.996	22.4	521.6	4951.7002	10000	0.1280	8.028E-3	6189.6	6.1896E5	3.384E-3	0.3	2.8	170.996	341.75	203.9
106.1	247.3	0.4290	20.996	22.4	506.7	5195.5698	10000	0.1244	8.287E-3	6494.5	6.4945E5	3.384E-3	0.3	2.9	171.996	325.45	197.8
101.8	242.1	0.4204	21.996	22.4	509.2	5358.8501	10000	0.1250	8.684E-3	6698.6	6.6986E5	3.384E-3	0.4	2.9	172.996	312.35	193.7
96.36	234.3	0.4112	22.996	22.4	534.8	5596.7900	10000	0.1313	9.739E-3	6996.0	6.9960E5	3.384E-3	0.4	2.9	173.996	295.62	187.5
93.62	229.3	0.4082	23.996	22.4	529.9	5746.5498	10000	0.1301	0.01007	7183.2	7.1832E5	3.384E-3	0.4	2.9	174.996	287.23	183.5
90.13	221.6	0.4067	25.000	22.4	548.9	5972.1099	10000	0.1347	0.01118	7465.1	7.4651E5	3.383E-3	0.4	2.9	176.000	276.52	177.3
85.32	216.3	0.3944	25.996	22.4	543.9	6124.0098	10000	0.1335	0.01162	7655.0	7.6550E5	3.383E-3	0.4	2.9	176.996	261.76	173.1
81.64	211.2	0.3865	27.000	22.4	534.8	6258.1201	10000	0.1313	0.01199	7822.7	7.8227E5	3.383E-3	0.5	3.0	178.000	250.45	169.0
77.57	203.5	0.3811	27.996	22.4	546.4	6464.9302	10000	0.1341	0.01319	8081.2	8.0812E5	3.383E-3	0.5	3.0	178.996	237.98	162.8
74.17	198.2	0.3741	28.996	22.4	543.9	6601.5898	10000	0.1335	0.01384	8252.0	8.2520E5	3.383E-3	0.5	3.0	179.996	227.54	158.6
71.03	192.9	0.3682	29.996	22.4	544.8	6732.6401	10000	0.1337	0.01464	8415.8	8.4158E5	3.383E-3	0.5	3.0	180.996	217.92	154.3
66.66	185.3	0.3598	30.996	22.4	552.2	6920.0200	10000	0.1355	0.01609	8650.0	8.6500E5	3.384E-3	0.5	3.0	181.996	204.52	148.2
62.85	180.0	0.3492	31.996	22.4	563.8	7045.8301	10000	0.1384	0.01740	8807.3	8.8073E5	3.384E-3	0.5	3.0	182.996	192.82	144.0
58.45	172.2	0.3395	32.996	22.4	567.1	7219.4600	10000	0.1392	0.01913	9024.3	9.0243E5	3.384E-3	0.5	3.1	183.996	179.33	137.7
55.68	167.1	0.3333	33.992	22.4	556.3	7331.7300	10000	0.1365	0.01994	9164.7	9.1647E5	3.383E-3	0.6	3.1	184.992	170.82	133.6
52.22	161.8	0.3228	34.996	22.4	553.9	7444.4600	10000	0.1359	0.02116	9305.6	9.3056E5	3.384E-3	0.6	3.1	185.996	160.21	129.4
48.34	153.7	0.3146	35.996	22.4	567.9	7606.7402	10000	0.1394	0.02405	9508.4	9.5084E5	3.384E-3	0.6	3.1	186.996	148.30	122.9
45.52	148.6	0.3064	36.996	22.4	571.2	7705.7998	10000	0.1402	0.02588	9632.3	9.6323E5	3.384E-3	0.6	3.1	187.996	139.66	118.9
43.55	143.3	0.3040	37.996	22.4	572.0	7805.4102	10000	0.1404	0.02786	9756.8	9.7568E5	3.383E-3	0.6	3.1	188.996	133.62	114.6
39.08	135.2	0.2892	38.996	22.4	575.3	7948.6001	10000	0.1412	0.03150	9935.8	9.9358E5	3.384E-3	0.6	3.2	189.996	119.90	108.1
37.64	130.1	0.2894	39.996	22.4	571.2	8035.6802	10000	0.1402	0.03376	10045	1.0045E6	3.384E-3	0.7	3.2	190.996	115.47	104.1
34.19	124.8	0.2740	40.996	22.4	602.6	8122.7998	10000	0.1479	0.03870	10154	1.0154E6	3.384E-3	0.7	3.2	191.996	104.89	99.82
32.02	116.6	0.2746	41.996	22.4	594.4	8247.0898	10000	0.1459	0.04371	10309	1.0309E6	3.384E-3	0.7	3.2	192.996	98.244	93.29
28.95	111.6	0.2595	42.996	22.4	601.8	8321.6699	10000	0.1477	0.04836	10402	1.0402E6	3.384E-3	0.7	3.2	193.996	88.805	89.24
26.41	106.3	0.2486	43.996	22.4	599.3	8396.2100	10000	0.1471	0.05308	10495	1.0495E6	3.384E-3	0.7	3.2	194.996	81.033	85.01
24.74	100.7	0.2457	44.996	22.4	583.6	8470.6104	10000	0.1432	0.05757	10588	1.0588E6	3.384E-3	0.7	3.3	195.996	75.903	80.55
21.60	92.50	0.2335	45.996	22.4	594.4	8569.8203	10000	0.1459	0.06947	10712	1.0712E6	3.384E-3	0.8	3.3	196.996	66.273	74.00
19.37	87.16	0.2223	46.996	22.4	593.5	8632.1602	10000	0.1457	0.07813	10790	1.0790E6	3.384E-3	0.8	3.3	197.996	59.436	69.73
16.95	81.48	0.2081	47.996	22.4	591.1	8693.6699	10000	0.1451	0.08904	10867	1.0867E6	3.384E-3	0.8	3.3	198.996	52.008	65.18
15.15	73.13	0.2072	48.996	22.4	605.9	8774.3604	10000	0.1487	0.1133	10968	1.0968E6	3.384E-3	0.8	3.3	199.996	46.486	58.50
12.41	67.70	0.1833	49.996	22.4	589.4	8823.2402	10000	0.1447	0.1286	11029	1.1029E6	3.384E-3	0.8	3.3	200.996	38.066	54.16
10.59	61.82	0.1714	51.000	22.4	606.8	8872.4199	10000	0.1489	0.1588	11091	1.1091E6	3.384E-3	0.9	3.4	202.000	32.503	49.45
9.209	55.77	0.1651	51.996	22.4	608.4	8915.4805	10000	0.1493	0.1956	11144	1.1144E6	3.384E-3	0.9	3.4	202.996	28.252	44.62
7.685	50.40	0.1525	52.996	22.4	601.0	8952.4404	10000	0.1475	0.2366	11191	1.1191E6	3.384E-3	0.9	3.4	203.996	23.579	40.32
6.405	44.41	0.1442	53.992	22.4	606.8	8988.6201	10000	0.1489	0.3076	11236	1.1236E6	3.384E-3	0.9	3.4	204.992	19.650	35.53
4.763	37.56	0.1268	54.996	22.4	605.1	9024.8799	10000	0.1485	0.4290	11281	1.1281E6	3.384E-3	0.9	3.4	205.996	14.613	30.04
3.713	31.49	0.1179	55.996	22.4	606.8	9049.1201	10000	0.1489	0.6120	11311	1.1311E6	3.383E-3	0.9	3.4	206.996	11.392	25.19
2.368	24.93	0.09498	56.996	22.4	615.9	9072.5801	10000	0.1512	0.9911	11341	1.1341E6	3.384E-3	0.9	3.5	207.996	7.2638	19.94
1.420	17.59	0.08076	57.992	22.4	604.3	9089.9404	10000	0.1483	1.953	11362	1.1362E6	3.384E-3	1.0	3.5	208.992	4.3579	14.07
1.059	14.79	0.07160	58.996	22.4	613.4	9095.6699	10000	0.1505	2.804	11370	1.1370E6	3.383E-3	1.0	3.5	209.996	3.2490	11.83
0.3993	8.311	0.04804	59.996	22.4	607.6	9103.7998	10000	0.1491	8.796	11380	1.1380E6	3.384E-3	1.0	3.5	210.996	1.2250	6.649

